HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1,2,2-Trichlorocyclopropane-1-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 14299770 | HCID 14299770 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 1,2,2-Trichlorocyclopropane-1-carbonyl chloride | HCID 14299772 | — |
Reaction Steps
Thionyl chloride (50 ml) was added to a solution of 1,2,2-trichlorocyclopropane carboxylic acid (47.4 grams) in 300 ml of benzene. The reaction mixture was heated to reflux temperature and stirred for approximately 20 hours. The solvents were evaporated in vacuo to provide the intermediate acid chloride derivative, 1,2,2-trichlorocyclopropane carboxylic acid chloride (43.8 grams).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04704156 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-f1e80488b731468fb8f34a1371877a1d |
| Source note | uspto-grants-1987_11 |