Hydrochloric Acid → HCID 21464694, compound

Participants

Reaction Steps

0.2 moles (8 ml) methanol, 0.15 moles (12 ml) pyridine and 50 ml toluene were put in a 100-ml beaker with a magnetic stirrer, and the crude product as per (b) was (1,4,6-trimethylcyclohex-3-en-1-carboxylic acid chloride) added dosewise with vigorous stirring. The reaction mixture was stirred for another hour at room temperature and then 25 ml water and 5 ml concentrated hydrochloric acid were added to it. Then the phases were separated, the organic phase dried with sodium sulfate and distilled via the Vigreux column after removal of the solvent.

Provenance & Evidence