HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13577265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methyl-4-phenylpentanol | HCID 3021997 | — |
| Product | HCID 13577265 | HCID 13577265 | 62.1% |
Reaction Steps
219 g of 2,4-dimethyl-4-phenyl-butan-1-ol are added dropwise to 161 g of thionyl chloride, the mixture is stirred overnight at room temperature and then for 2 hours at 140° C., and the crude product is distilled to give 150 g of 2,4-dimethyl-4-phenylbutyl chloride of boiling point 84°-86° C./0.1 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04705553 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-6a8c4697cb6c4c01ad7c1c4e0fa95d47 |
| Source note | uspto-grants-1987_11 |