2,6-Dimethylmorpholine, cis- → HCID 13577276, compound

Participants

Reaction Steps

20 g of 2-methyl-5-phenylpentyl chloride and 35 g of 2,6-cis-dimethylmorpholine are heated at 150° C. for 10 hours, after which the mixture is left to cool, taken up with CH2Cl2, washed with water, dilute NaOH and once again with water, dried over Na2SO4 and evaporated down, and the residue is distilled to give 18 g of a product of boiling point 130°-132° C./0.4 mbar.

Provenance & Evidence