Bromochloromethane → HCID 11658340, compound

Participants

Reaction Steps

Triethylamine (40 mmol) was added to a mixture of 2-mercapto-1-methylimidazole (40 mmol) and bromochloromethane (0.8 mol). The mixture was stirred for 1 hour at room temperature, washed with water and the dried (MgSO4) solution evaporated. Yield: 5.85 g (90%). 1H NMR (CDCl3, δ): 3.77 (CH3), 5.00 (CH2), 6.7-7.2 (H-4 and H-5). The product was used in the succeeding step without further purification.

Provenance & Evidence