HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 5-[5-(3-phenylpropyl)thiophen-2-yl]pentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Eprovafen | HCID 208926 | — |
| Product | Ethyl 5-[5-(3-phenylpropyl)thiophen-2-yl]pentanoate | HCID 15667456 | — |
Reaction Steps
3 g of 5-[5-(3-phenylpropyl)-thien-2-yl]-valeric acid are dissolved in 10 ml of ethanol and the solution is saturated with HCl gas. The solution is stirred at room temperature for 24 hours and concentrated in vacuo. Purification by column chromatography (silica gel/hexane/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04705802 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-0fcece9982ff482b8168ceb731d814e4 |
| Source note | uspto-grants-1987_11 |