HRID247303

反应详情

EQUATION

反应方程式

HRID 247303 的结构方程式

PROCEDURE

实验过程

Following the procedure of Example 1, 4-benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-one and dimethylamine were reacted and the free base of the title compound was obtained in the concentrated residue. Recrystallization from ethanol-water gave the product, m.p. 75°-77° C.

WORKUP

后处理

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