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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 247303Generated: October 30, 2026

Dimethylamine → HCID 13726314, compound

https://huagongshe.com/reaction/247303

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
Reactant4-Benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-oneHCID 13726292—
ProductHCID 13726314HCID 13726314—

Reaction Steps

Following the procedure of Example 1, 4-benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-one and dimethylamine were reacted and the free base of the title compound was obtained in the concentrated residue. Recrystallization from ethanol-water gave the product, m.p. 75°-77° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04705853
Source datasetuspto-grants-1987_11
ORD IDord-7c399d1b78d3492b8ebceaa87c7474fa
Source noteuspto-grants-1987_11