反应详情

3-(3,5-Difluorophenyl)propylazide (0.034 mol) in methanol (75 ml) was shaken with a slurry of methanol washed Raney nickel under 50 psi hydrogen for 2 hours. The reaction mixture was filtered and the filtrate concentrated to yield 5.6 g (96%) of an oily product.

1. washwashed Raney nickel under 50 psi hydrogen for 2 hours
2. filtrationThe reaction mixture was filtered
3. concentrationthe filtrate concentrated