HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 3,5-Difluoro-4-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 3,5-Difluoro-4-methoxybenzonitrile | HCID 10583253 | — |
| Product | 3,5-Difluoro-4-methoxybenzaldehyde | HCID 14450860 | — |
Reaction Steps
3,5-Difluoro-4-methoxybenzonitrile (0.237 mol), Raney alloy (40 g) and 90% formic acid (400 ml) were reacted substantially as described in Example 7A above to obtain 22.9 g (56%) of a white, low melting solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04707488 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-e47acd577b1744ea8d641753afdbd575 |
| Source note | uspto-grants-1987_11 |