HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 20160706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 20160682 | HCID 20160682 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20160706 | HCID 20160706 | — |
Reaction Steps
3-Acetyl-7-chlorosulfonyl-8-methoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine (3.9 g, 0.01 m) is dissolved in methylene chloride (50 ml) and added to concentrated ammonium hydroxide (15 ml), then stirred and filtered to give 3-acetyl-8-methoxy-1-phenyl-7-sulfamoyl-2,3,4,5-tetrahydro-1H-3-benzazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04707483 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-f1a16549fb684b3bbc207623c6133877 |
| Source note | uspto-grants-1987_11 |