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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 247445Generated: October 30, 2026

Thionyl Chloride → HCID 20160730, compound

https://huagongshe.com/reaction/247445

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantChlorosulfonic acidHCID 24638—
ReactantHCID 68116039HCID 68116039—
ProductHCID 20160730HCID 20160730—

Reaction Steps

Following the general procedure of Example 2, 7-methoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine maleate is acetylated and treated with chlorosulfonic acid followed by thionyl chloride to give 3-acetyl-8-chlorosulfonyl-7-methoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04707483
Source datasetuspto-grants-1987_11
ORD IDord-168a6b9a0d66476e899945b02b80bbff
Source noteuspto-grants-1987_11