m-Chloroperbenzoic acid → HCID 20160906, compound

HRID 247459Notes

Reaction equation

HRID 247459 reaction equation
[C:1]1([CH:7]([CH2:10][CH3:11])[C:8]#[N:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.ClC1C=CC=[C:15]([C:19]([O:21]O)=O)[CH:14]=1>>[CH2:10]([C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([CH2:14][CH:15]1[CH2:19][O:21]1)[C:8]#[N:9])[CH3:11]

Participants

3

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 95334Benzeneacetonitrile, .alpha.-ethyl-

Product 1

HCID 20160906HCID 20160906, compound

Procedure

The title compound was prepared by the methods described in Examples 2 and 3 except that 2-phenylbutyronitrile was used instead of methyl 2-phenylbutyrate and complete epoxidation required adding a second quantity of m-chloroperbenzoic acid. The resultant light-yellow oil was used in subsequent reactions without furher purification.

Workup

  1. customThe resultant light-yellow oil was used in subsequent reactions without furher purification

Sources & evidence

ORD record
ord-a41c669c11d44db29915a2c164770dfb
Source dataset
uspto-grants-1987_11
Patent number
US04707499

Reaction notes

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