HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hydroxybenzotriazole → HCID 178485470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733207 | — |
| Reactant | Methylamine hydrochloride | HCID 6364545 | — |
| Reactant | 4-[[(Z)-(2-oxo-1H-indol-3-ylidene)-phenylmethyl]amino]benzoic acid | HCID 178517088 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178485470 | HCID 178485470 | — |
Reaction Steps
Prepared analogously to Example 18 from (Z)-3-[1-(4-carboxyphenylamino)-1-phenyl-methylidene]-2-indolinone, methylamine-hydrochloride, TBTU, HOBt and N-ethyl-N,N-diisopropylamine in DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06855710B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-e3ae603ae8a94acf81fde332878092f2 |
| Source note | uspto-grants-2005_02 |