HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178450967, compound → HCID 178450964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178450967 | HCID 178450967 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178450964 | HCID 178450964 | 84.1% |
Reaction Steps
644 mg of the obtained N-benzyloxycarbonyl-glycyl-D,L-argininal dibutyl acetal was dissolved in 30 ml of methanol and subjected to catalytic reduction with palladium black for four hours. After the completion of the reaction, the palladium black was removed and the solvent was distilled off in vacuo to give 390 mg of glycyl-D,L-argininal dibutyl acetal in the form of a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04708944 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-95008bdc196f43f2ba607d2b3e869606 |
| Source note | uspto-grants-1987_11 |