HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178450966, compound → HCID 178450965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178450966 | HCID 178450966 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178450965 | HCID 178450965 | 136.1% |
Reaction Steps
132 mg of the N-benzyloxycarbonyl-D-valyl-glycyl-D,L-argininal dibutyl acetal was dissolved in 10 ml of methanol and subjected to catalytic reduction with palladium black for four hours. After the completion of the reaction, the palladium black was removed and the solvent was distilled off in vacuo to give 138 mg of D-valyl-glycyl-D,L-argininal dibutyl acetal in the form of a powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04708944 |
| Source dataset | uspto-grants-1987_11 |
| ORD ID | ord-864692f12bcd4d56a1a34fed322eba3b |
| Source note | uspto-grants-1987_11 |