참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | N-(4-Aminophenyl)propanamide | HCID 314342 | — |
| 반응물 | 3-(1-Ethoxy-1-phenyl-methylidene)-2-indolinone | HCID 54037623 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178460035 | HCID 178460035 | — |
반응 단계
265 mg (1 mmol) of 3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone are dissolved in 5 ml of DMF and after the addition of 300 mg (1.8 mmol) of 4-propionylamino-aniline stirred for 8 hours at 150° C. After cooling, it is diluted with water, the crystalline product is suction filtered, washed and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06855710B2 |
|---|
| 출처 데이터셋 | uspto-grants-2005_02 |
|---|
| ORD ID | ord-46821cce08f7485c9c9fe6008bf62fa5 |
|---|
| 출처 메모 | uspto-grants-2005_02 |
|---|
