HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11780934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-Methyl-N-{1-[4-(p-fluorophenoxy)butyl]-4-piperidyl}acetamide | HCID 19764643 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11780934 | HCID 11780934 | — |
Reaction Steps
0.05 mole of the compound obtained in stage D is refluxed for 12 hours in the presence of 570 cm3 of methanol and 340 cm3 of 5N hydrochloric acid. The methanol is evaporated and the mixture is poured into ice and then basified with sodium hydroxide. It is extracted with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208243 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-c01548b052cb476bb7336025740cb417 |
| Source note | uspto-grants-1993_05 |