HRID247845

反应详情

EQUATION

反应方程式

HRID 247845 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

0.05 mole of the compound obtained in stage D is refluxed for 12 hours in the presence of 570 cm3 of methanol and 340 cm3 of 5N hydrochloric acid. The methanol is evaporated and the mixture is poured into ice and then basified with sodium hydroxide. It is extracted with ether.

WORKUP

后处理

  1. customThe methanol is evaporated
  2. additionthe mixture is poured into ice
  3. extractionIt is extracted with ether