HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 149069-42-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 19764635 | HCID 19764635 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 149069-42-1 | HCID 67859279 | — |
Reaction Steps
0.05 mole of the compound obtained in stage C in 130 cm3 of ethanol and 3 cm3 of acetic acid is hydrogenated in the presence of 1.3 g of palladium dihydroxide at 50° C. and at a pressure of 5 kilograms/cm2. The mixture is evaporated and then filtered. 12 g of the expected compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208243 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-cd24122224ea4b31961bdb6e13ad2975 |
| Source note | uspto-grants-1993_05 |