Ethanol → 149069-42-1

HRID 247851Notes

Reaction equation

HRID 247851 reaction equation
[CH3:1][N:2]([CH2:6][CH:7]1[CH2:11][CH2:10][N:9](CC2C=CC=CC=2)[CH2:8]1)[C:3](=[O:5])[CH3:4].C([OH:21])C>C(O)(=O)C.[OH-].[OH-].[Pd+2]>[C:3]([OH:5])(=[O:21])[CH3:4].[CH3:1][N:2]([CH2:6][CH:7]1[CH2:11][CH2:10][NH:9][CH2:8]1)[C:3](=[O:5])[CH3:4]

Participants

5

Reactant 2

HCID 702EthanolHCID 19764635HCID 19764635, compound

Product 1

HCID 67859279149069-42-1

Reagents, catalysts & solvents 2

HCID 9942167Palladium hydroxideCatalystHCID 176Acetic AcidSolvent

Procedure

0.05 mole of the compound obtained in stage C in 130 cm3 of ethanol and 3 cm3 of acetic acid is hydrogenated in the presence of 1.3 g of palladium dihydroxide at 50° C. and at a pressure of 5 kilograms/cm2. The mixture is evaporated and then filtered. 12 g of the expected compound are obtained.

Workup

  1. customThe mixture is evaporated
  2. filtrationfiltered

Sources & evidence

ORD record
ord-cd24122224ea4b31961bdb6e13ad2975
Source dataset
uspto-grants-1993_05
Patent number
US05208243

Reaction notes

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