HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 247917Generated: October 25, 2026
Methyl iodide → 2-[[(2-Methoxybenzoyl) [4-(tetradecyloxy)benzoyl]amino]methyl]-1-methylpyridinium iodide
https://huagongshe.com/reaction/247917
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-Methoxy-N-(2-pyridinylmethyl)-N-[4-(tetradecyloxy)benzoyl]benzamide | HCID 19016434 | — |
| Product | 2-[[(2-Methoxybenzoyl) [4-(tetradecyloxy)benzoyl]amino]methyl]-1-methylpyridinium iodide | HCID 67878949 | — |
Reaction Steps
A mixture of 0.770 g of product from Example 6 and 4.29 ml methyl iodide is heated in a sealed tube at 105° C. for 15 hours. The cooled reaction is concentrated in vacuo to give 0.960 g of the desired product as a thick yellow oil which solidified on standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05208247 |
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| Source dataset | uspto-grants-1993_05 |
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| ORD ID | ord-8162f06ca7e64419b0505c424ce402f8 |
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| Source note | uspto-grants-1993_05 |
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