Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 10434714 | HCID 10434714 | — |
| Product | HCID 10008845 | HCID 10008845 | — |
Reaction Steps
A mixture of 0.281 g of product from Example 27 and 1.88 ml of methyl iodide is heated in a sealed tube at 110° C. for 20 hours. The cooled solution is concentrated in vacuo and the residue recrystallized from methyl alcohol to give 0.367 g of the desired product as cream crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05208247 |
|---|
| Source dataset | uspto-grants-1993_05 |
|---|
| ORD ID | ord-5c3eb44083e14daa8978b2145522b206 |
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| Source note | uspto-grants-1993_05 |
|---|
