HRID247951

反应详情

EQUATION

反应方程式

HRID 247951 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 32 using 60 g of product from Example 41, 480 ml methyl alcohol, 190 ml of ethyl alcohol, 28.5 ml of water and 26.7 g of potassium hydroxide. The residue is recrystallized from chloroform/hexane to give 47 g of the desired product as white crystals.

WORKUP

后处理

  1. customThe residue is recrystallized from chloroform/hexane