HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 4-Methoxy-3-(tetradecyloxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-Methoxy-3-(tetradecyloxy)benzoic acid methyl ester | HCID 53639315 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-Methoxy-3-(tetradecyloxy)benzoic acid | HCID 19015135 | 81.3% |
Reaction Steps
The title compound is prepared by the procedure of Example 32 using 60 g of product from Example 41, 480 ml methyl alcohol, 190 ml of ethyl alcohol, 28.5 ml of water and 26.7 g of potassium hydroxide. The residue is recrystallized from chloroform/hexane to give 47 g of the desired product as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-d563867407964208885ac774259a299f |
| Source note | uspto-grants-1993_05 |