HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13354737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 54425506 | HCID 54425506 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13354737 | HCID 13354737 | 83.1% |
Reaction Steps
The title compound is prepared by the procedure of Example 32 using 40 g of the product from Example 46, 320 ml of methyl alcohol, 125 ml ethyl alcohol, 20 ml of water and 17.8 g of potassium hydroxide. The residue is recrystallized from chloroform/hexane to give 32 g of the desired product as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-c80d21e788f6413898e7a7b9c4dde8a9 |
| Source note | uspto-grants-1993_05 |