HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-Methyl-2-[[[[4-(tetradecyloxy)phenyl]acetyl]amino]methyl]pyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-(2-Pyridinylmethyl)-4-(tetradecyloxy)benzeneacetamide | HCID 10365880 | — |
| Product | 1-Methyl-2-[[[[4-(tetradecyloxy)phenyl]acetyl]amino]methyl]pyridinium iodide | HCID 10031135 | 87.6% |
Reaction Steps
The title compound is prepared by the procedure of Example 28 using 1.0 g of product from Example 54 and 16.18 g of methyl iodide. The residue is recrystallized from methyl alcohol to give 1.16 g of the desired product as cream prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208247 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-d9a1a85cd6214c4d87c938ed980896e4 |
| Source note | uspto-grants-1993_05 |