HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 248005Generated: November 1, 2026
Methyl iodide → 2-[[Acetyl[[[4-(tetradecyloxy)phenyl]methoxy]carbonyl]amino]methyl]-1-methylpyridinium iodide
https://huagongshe.com/reaction/248005
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | [4-(Tetradecyloxy)phenyl]methyl acetyl(2-pyridinylmethyl)carbamate | HCID 9983311 | — |
| Product | 2-[[Acetyl[[[4-(tetradecyloxy)phenyl]methoxy]carbonyl]amino]methyl]-1-methylpyridinium iodide | HCID 10349150 | 93.7% |
Reaction Steps
A mixture of 1.37 g of product from Example 96 and 19.55 g of methyl iodide is heated in a sealed tube at 100° C. for 5 hours. The reaction is concentrated in vacuo and the residue recrystallized from methyl alcohol to give 1.65 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05208247 |
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| Source dataset | uspto-grants-1993_05 |
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| ORD ID | ord-038f003302c643be86b1536f6955fe6d |
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| Source note | uspto-grants-1993_05 |
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