huagongshe.com
HRID248098

反应详情

EQUATION

反应方程式

HRID 248098 的结构方程式

REACTANTS

反应物

2
结构：COC1(c2cccc(S)c2)CCOCC1
HCID19375715

未命名化合物

结构：CC1(C)c2ccc(I)cc2C(C)(C)S1(=O)=O
HCID19764866

未命名化合物

PRODUCTS

生成物

1
结构：COC1(c2cccc(Sc3ccc4c(c3)C(C)(C)S(=O)(=O)C4(C)C)c2)CCOCC1
HCID19764772

未命名化合物

收率 28%

PROCEDURE

实验过程

Using a similar procedure to that described in Example 12, 5-iodo-1,1,3,3-tetramethyl-1,3-dihydrobenzo[c]thiophene-2,2-dioxide was reacted with 4-(3-mercaptophenyl)-4-methoxytetrahydropyran to give 4-methoxy-4-[3-(1,1,3,3-tetramethyl-2,2-dioxo-1,3-dihydrobenzo[c]thien-5-ylthio)phenyl]tetrahydropyran in 28% yield, m.p. 133°-135° C.