1-Iodopropane → HCID 73653193, compound

Participants

Reaction Steps

To a solution of 3-(3-pyridinyl)-1-phenylpropan-1-one oxime (4.79 g, 0.021 mol) in acetonitrile (50 mL) was added 1-iodopropane (3.10 mL, 0.032 mol). The mixture was then refluxed for 12 hours. Solvent was removed to dryness under vacuum to give a dark brown oil (8.46 g, 100%). The crude product was used in the next step without further purification.

Provenance & Evidence