HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → Ethyl 3-(hexadecylthio)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Hexadecanethiol | HCID 18015 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Ethyl 3-(hexadecylthio)propanoate | HCID 19764352 | 184.3% |
Reaction Steps
A solution of 15 g of hexadecylmercaptan, 3.0 g of ethyl acrylate and 2 ml of triethylamine is stirred at ambient temperature for 18 hours. The solvent is evaporated and the concentrate purified by high pressure liquid chromatography, to give 19.8 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05208223 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-46a26e1746954432a89f22281af2d4ff |
| Source note | uspto-grants-1993_05 |