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HRID248169

反应详情

EQUATION

反应方程式

HRID 248169 的结构方程式

REACTANTS

反应物

2
结构：C=CC(=O)OCC
HCID8821

Ethyl acrylate

C5H8O2

结构：CCCCCCCCCCCCCCCCS
HCID18015

1-Hexadecanethiol

C16H34S

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCCSCCC(=O)OCC
HCID19764352

未命名化合物

收率 184.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

A solution of 15 g of hexadecylmercaptan, 3.0 g of ethyl acrylate and 2 ml of triethylamine is stirred at ambient temperature for 18 hours. The solvent is evaporated and the concentrate purified by high pressure liquid chromatography, to give 19.8 g of the desired product.

WORKUP

后处理

  1. customThe solvent is evaporated
  2. customthe concentrate purified by high pressure liquid chromatography