HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178439713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 2-Propylpropanediol | HCID 21943838 | — |
| Reactant | HCID 178520943 | HCID 178520943 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178439713 | HCID 178439713 | — |
Reaction Steps
A mixture of 0.02 mol of trans-4-trifluoromethyl-1-formylcyclohexane (prepared as in Example 3), 0.02 mol of 2-propylpropanediol, 30 ml of toluene and 0.5 g of pTsOH (sic) is heated for 4 hours on a water separator. The pure product is obtained after customary work-up and crystallization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05209868 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-08f48b11c11f42c2b6f50a89daae7568 |
| Source note | uspto-grants-1993_05 |