tert-butyl N-[(4-aminophenyl)methyl]-N-methylcarbamate → HCID 178482861, compound

HRID 24834Notes

Reaction equation

HRID 24834 reaction equation
C(O[C:4](=[C:11]1[C:19]2[C:14](=[CH:15][CH:16]=[C:17]([N+:20]([O-:22])=[O:21])[CH:18]=2)[NH:13][C:12]1=[O:23])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)C.[C:24]([O:28][C:29]([N:31]([CH2:33][C:34]1[CH:40]=[CH:39][C:37]([NH2:38])=[CH:36][CH:35]=1)[CH3:32])=[O:30])([CH3:27])([CH3:26])[CH3:25]>CN(C=O)C>[C:24]([O:28][C:29]([N:31]([CH2:33][C:34]1[CH:40]=[CH:39][C:37]([NH:38]/[C:4](=[C:11]2\[C:12](=[O:23])[NH:13][C:14]3[C:19]\2=[CH:18][C:17]([N+:20]([O-:22])=[O:21])=[CH:16][CH:15]=3)/[C:5]2[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=2)=[CH:36][CH:35]=1)[CH3:32])=[O:30])([CH3:27])([CH3:25])[CH3:26]

Participants

4

Reactant 2

HCID 11637262tert-butyl N-[(4-aminophenyl)methyl]-N-methylcarbamateHCID 537348873-(1-Ethoxy-1-phenylmethylidene)-5-nitro-2-indolinone

Product 1

HCID 178482861HCID 178482861, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared analogously to Example 89 from 3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone and 4-(N-tert.butoxycarbonyl-N-methyl-amino)methyl-aniline in DMF.

Sources & evidence

ORD record
ord-430c0f219253423a8b9a2ceb549f2955
Source dataset
uspto-grants-2005_02
Patent number
US06855710B2

Reaction notes

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