反应详情

温度

55 °C

A mixture of 55 g of selenium dioxide, 11 ml of water and 150 ml of dioxane was heated at 55° C. until solution was complete. A 55 g portion of 2-acetylfuran was added, the mixture was refluxed for 4 hours, then filtered and evaporated. The residue was dissolved in dichloromethane, treated with activated charcoal, filtered and evaporated. The residue was distilled, giving 28 g of α-oxo-2-furanacetaldehyde.

1. temperaturethe mixture was refluxed for 4 hours
2. filtrationfiltered
3. customevaporated
4. dissolutionThe residue was dissolved in dichloromethane
5. additiontreated with activated charcoal
6. filtrationfiltered
7. customevaporated
8. distillationThe residue was distilled