HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 131717905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 23042966 | HCID 23042966 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131717905 | HCID 131717905 | — |
Reaction Steps
A 54 mg portion of the base compound from Example 128 was dissolved, with heat, in a mixture of ethanol, chloroform and a little dimethylformamide. A few drops of concentrated hydrochloric acid were added, the solid was collected, washed with water, ether and dried, giving 35 mg of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05210193 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-e7ea54ae83e0496f99beb7c0cc5ad309 |
| Source note | uspto-grants-1993_05 |