Hydrazine hydrate (1:1) → HCID 178509831, compound

HRID 24861Notes

Reaction equation

HRID 24861 reaction equation
[C:1]1([NH:7]/[C:8](=[C:27]2\[C:28](=[O:39])[NH:29][C:30]3[C:35]\2=[CH:34][C:33]([N+:36]([O-:38])=[O:37])=[CH:32][CH:31]=3)/[C:9]2[CH:14]=[CH:13][C:12]([CH2:15][N:16]3C(=O)C4=CC=CC=C4C3=O)=[CH:11][CH:10]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.O.NN>C(O)C>[C:1]1([NH:7]/[C:8](=[C:27]2\[C:28](=[O:39])[NH:29][C:30]3[C:35]\2=[CH:34][C:33]([N+:36]([O-:38])=[O:37])=[CH:32][CH:31]=3)/[C:9]2[CH:14]=[CH:13][C:12]([CH2:15][NH2:16])=[CH:11][CH:10]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 178517248HCID 178517248, compound

Product 1

HCID 178509831HCID 178509831, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 140 from (Z)-3-[1-phenylamino-1-(4-phthalimidomethyl-phenyl)-methylidene]-5-nitro-2-indolinone and hydrazine hydrate solution in ethanol.

Sources & evidence

ORD record
ord-da5a5c5f53de4276af6487df396d4199
Source dataset
uspto-grants-2005_02
Patent number
US06855710B2

Reaction notes

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