Methyl iodide → HCID 178482164, compound

HRID 24881Notes

Reaction equation

HRID 24881 reaction equation
[CH3:1][S:2]([NH:5][C:6]1[CH:7]=[C:8]([NH:12]/[C:13](=[C:20]2\[C:21](=[O:29])[NH:22][C:23]3[C:28]\2=[CH:27][CH:26]=[CH:25][CH:24]=3)/[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:9]=[CH:10][CH:11]=1)(=[O:4])=[O:3].CI.[C:32](=O)([O-])[O-].[K+].[K+]>CC(C)=O>[CH3:32][N:5]([C:6]1[CH:7]=[C:8]([NH:12]/[C:13](=[C:20]2\[C:21](=[O:29])[NH:22][C:23]3[C:28]\2=[CH:27][CH:26]=[CH:25][CH:24]=3)/[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:9]=[CH:10][CH:11]=1)[S:2]([CH3:1])(=[O:3])=[O:4]

Participants

5

Reactant 3

HCID 6328Methyl iodideHCID 11430Potassium CarbonateHCID 178505022HCID 178505022, compound

Product 1

HCID 178482164HCID 178482164, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Prepared analogously to Example 36 from (Z)-3-[1-(3-methylsulphonylamino-phenylamino)-1-phenyl-methylidene]-2-indolinone, methyliodide and potassium carbonate in acetone.

Sources & evidence

ORD record
ord-3271d3d3a10447819a002ed62c0cb0b5
Source dataset
uspto-grants-2005_02
Patent number
US06855710B2

Reaction notes

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