HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 19689901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 19690047 | HCID 19690047 | — |
| Product | HCID 19689901 | HCID 19689901 | 77.9% |
Reaction Steps
Using 4-amino-3-methoxy-N-{2-[4-(4-fluorobenzoyl)piperidino]ethyl}-N-(3-methoxyphenyl)benzamide (253.0 mg, 0.50 mmol) and acetic anhydride (0.095 ml, 1.00 mmol), the procedure of inventive Example 94 was repeated to obtain 213.0 mg (77.9%) of the title compound in a yellow amorphous form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-36584347913d4b168f2b2a55aee4be5c |
| Source note | uspto-grants-1998_03 |