HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → hexahydro-cyclopenta[b]furan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 15222216 | HCID 15222216 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | hexahydro-cyclopenta[b]furan-2-one | HCID 11665410 | — |
Reaction Steps
The compound (51) (12.6 g) was reduced with sodium borohydride (1.25 g) in methanol (400 ml) at 0° C. to give the titled compound (52). Yield: 12.1 g (95.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05212324 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-28223cfe1a7244de82a44afb1dbd7311 |
| Source note | uspto-grants-1993_05 |