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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 249144Generated: October 29, 2026

Oxalyl chloride → Bis(3-isobutylphenyl)chloromethane

https://huagongshe.com/reaction/249144

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
ReactantBis(3-isobutylphenyl)methanolHCID 19024807—
SolventDichloromethaneHCID 6344—
ProductBis(3-isobutylphenyl)chloromethaneHCID 19024840—

Reaction Conditions

Temperature25 °C

Reaction Steps

A mixture of bis(3-isobutylphenyl)methanol (2.87 g) and oxalyl chloride (1 ml) in dichloromethane (10 ml) was stirred at 25° C. for 2 hours. After evaporation of the solvent, the oily residue was distilled to give bis(3-isobutylphenyl)chloromethane (2.45 g) as pale yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05212320
Source datasetuspto-grants-1993_05
ORD IDord-0042c04ec38442f19ca8bf2ed8f8c9f5
Source noteuspto-grants-1993_05