HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 249144Generated: October 29, 2026
Oxalyl chloride → Bis(3-isobutylphenyl)chloromethane
https://huagongshe.com/reaction/249144
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Bis(3-isobutylphenyl)methanol | HCID 19024807 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Bis(3-isobutylphenyl)chloromethane | HCID 19024840 | — |
Reaction Steps
A mixture of bis(3-isobutylphenyl)methanol (2.87 g) and oxalyl chloride (1 ml) in dichloromethane (10 ml) was stirred at 25° C. for 2 hours. After evaporation of the solvent, the oily residue was distilled to give bis(3-isobutylphenyl)chloromethane (2.45 g) as pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05212320 |
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| Source dataset | uspto-grants-1993_05 |
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| ORD ID | ord-0042c04ec38442f19ca8bf2ed8f8c9f5 |
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| Source note | uspto-grants-1993_05 |
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