HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexane → HCID 15029369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexane | HCID 8078 | — |
| Reactant | HCID 18961685 | HCID 18961685 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15029369 | HCID 15029369 | 46.2% |
Reaction Steps
Tetrabutylammonium 2-(1-cyano-4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)nicotinate (0.36 g, 0.00068 mol) is placed into a mixture of cyclohexane and ethyl acetate for 3 months. The mixture is filtered to yield the title compound as a tan solid (0.09 g, 42%), mp 150°-153° C., identified by IR and NMR spectral analyses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05213607 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-769c0544ba124029ab8823c01fd5387d |
| Source note | uspto-grants-1993_05 |