HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 7-Octyl-2-fluorenecarbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 7-Octyl-2-fluorenecarboxylic acid | HCID 19760656 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 7-Octyl-2-fluorenecarbonyl chloride | HCID 19760665 | — |
Reaction Steps
To 0.70 g (2.17 mM) of 7-octyl-2-fluorenecarboxylic acid, 2.1 ml of thionyl chloride and a drop of N,N-dimethylformamide (DMF) were added, followed by heat-refluxing for 20 minutes under stirring. After the reaction, an excessive thionyl chloride was distilled-off under reduced pressure to obtain 7-octyl-2-fluorenecarbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05213709 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-bdc31afe4ec04e90a1722c547477e910 |
| Source note | uspto-grants-1993_05 |