HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 14372663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-(2-Methylpropyl)-1,2-benzenediol | HCID 14372665 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 14372663 | HCID 14372663 | — |
Reaction Steps
The same procedures as described in Example 8 were carried out by using 4.16 g (25 mM) of 4-isobutylcatechol, 5.06 g (50 mM) of triethylamine and 3.50 g (28 mM) of oxalyl chloride. 6-iso-Butyl-1,4-benzodioxine- 2,3-dione 2/5 hydrate was obtained in the yield of 5.11 g (22.5 mM) as colorless crystals having a melting point of 92°-97° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05214034 |
| Source dataset | uspto-grants-1993_05 |
| ORD ID | ord-858aee3f5549421a9669a0b3f4c89729 |
| Source note | uspto-grants-1993_05 |