Oxalyl chloride → HCID 14372663, compound

HRID 249266Notes

Reaction equation

HRID 249266 reaction equation
[CH2:1]([C:5]1[CH:6]=[C:7]([OH:12])[C:8](=[CH:10][CH:11]=1)[OH:9])[CH:2]([CH3:4])[CH3:3].[C:13](Cl)(=[O:17])[C:14](Cl)=[O:15]>C(N(CC)CC)C>[CH2:1]([C:5]1[CH:11]=[CH:10][C:8]2[O:9][C:13](=[O:17])[C:14](=[O:15])[O:12][C:7]=2[CH:6]=1)[CH:2]([CH3:4])[CH3:3]

Participants

4

Reactant 2

HCID 65578Oxalyl chlorideHCID 143726654-(2-Methylpropyl)-1,2-benzenediol

Product 1

HCID 14372663HCID 14372663, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The same procedures as described in Example 8 were carried out by using 4.16 g (25 mM) of 4-isobutylcatechol, 5.06 g (50 mM) of triethylamine and 3.50 g (28 mM) of oxalyl chloride. 6-iso-Butyl-1,4-benzodioxine- 2,3-dione 2/5 hydrate was obtained in the yield of 5.11 g (22.5 mM) as colorless crystals having a melting point of 92°-97° C.

Sources & evidence

ORD record
ord-858aee3f5549421a9669a0b3f4c89729
Source dataset
uspto-grants-1993_05
Patent number
US05214034

Reaction notes

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