HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 178515196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | Ethyl 4-chloro-6-fluoroquinoline-3-carboxylate | HCID 1479088 | — |
| Reactant | HCID 178515184 | HCID 178515184 | — |
| Product | HCID 178515196 | HCID 178515196 | — |
Reaction Steps
The title compound was prepared following the procedure described in Step 3 of the synthesis of 4a, using 3b and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm): 7.16 (1H, t, J=13.67 Hz), 7.41 (2H, t, J=7.56 Hz), 7.55 (1H, dt, J=8.54, 2.93 Hz), 7.77 (1H, dd, J=9.27, 4.88 Hz), 7.90 (1H, dd, J=9.27, 2.93 Hz), 8.18 (2H, dd, J=7.58, 1.95 Hz), 8.73 (1H, s). m/z 280.5 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863266B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-b6d4fbd1a61d466eae56dae3e2918e59 |
| Source note | uspto-grants-2011_01 |