HRID249676

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID268963

Ethyl 4-Chloroquinoline-3-carboxylate

C12H10ClNO2

HCID178469610

未命名化合物

PRODUCTS

生成物

HCID1511944

ethyl 4-chloro-6,7-difluoroquinoline-3-carboxylate

C12H8ClF2NO2

PROCEDURE

实验过程

The title compound was prepared following the procedure described in Step 2 for the synthesis of 3a using 2c instead of 2a. 1H NMR (CDCl3) δ (ppm): 1.47 (3H, t, J=7.08 Hz), 4.56 (2H, q, J=7.08 Hz), 7.72 (1H, d, J=8.79 Hz), 8.39 (1H, d, J=8.78 Hz), 9.23 (1H, s). m/z 271.6/273.6 (M+/M+2). m/z 272.6 (MH+).