Phenylhydrazine → HCID 178488062, compound

HRID 249678Notes

Reaction equation

HRID 249678 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[C:9]([O:12][CH3:13])[CH:10]=2)[N:5]=[CH:4][C:3]=1[C:14]([O:16]CC)=O.[C:19]1([NH:25][NH2:26])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH3:13][O:12][C:9]1[CH:8]=[CH:7][C:6]2[NH:5][CH:4]=[C:3]3[C:14](=[O:16])[N:25]([C:19]4[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=4)[N:26]=[C:2]3[C:11]=2[CH:10]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 304558Ethyl 4-chloro-6-methoxyquinoline-3-carboxylate

Product 1

HCID 178488062HCID 178488062, compound

Procedure

The title compound was prepared following the procedure described in Step 3 using 3d and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm): 3.90 (3H, s), 7.17 (1H, m), 7.27 (1H, dd, J=9.06, 2.64 Hz), 7.40 (2H, m), 7.57 (1H, d, J=3.02 Hz), 7.67 (1H, d, J=9.06 Hz), 8.20 (2H, m), 8.63 (1H, s). m/z 292.3 (MH+).

Sources & evidence

ORD record
ord-b8a2e6cb53f04124b4651771d5d79262
Source dataset
uspto-grants-2011_01
Patent number
US07863266B2

Reaction notes

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