Phenylhydrazine → HCID 178486989, compound

HRID 249679Notes

Reaction equation

HRID 249679 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][C:8]([O:12][CH3:13])=[CH:9][CH:10]=2)[N:5]=[CH:4][C:3]=1[C:14]([O:16]CC)=O.[C:19]1([NH:25][NH2:26])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH3:13][O:12][C:8]1[CH:9]=[CH:10][C:11]2[C:2]3[C:3]([C:14](=[O:16])[N:25]([C:19]4[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=4)[N:26]=3)=[CH:4][NH:5][C:6]=2[CH:7]=1

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 728976Ethyl 4-chloro-7-methoxyquinoline-3-carboxylate

Product 1

HCID 178486989HCID 178486989, compound

Procedure

The title compound was prepared following the procedure described in Step 3 using 3e and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm): 3.86 (3H, s), 7.10 (3H, m), 7.38 (2H, dd, J=8.24, 7.42 Hz), 8.09 (3H, m), 8.65 (1H, d, J=6.04 Hz). m/z 292.3 (MH+).

Sources & evidence

ORD record
ord-1b145d118b6b4810b0bbcf436b3e748f
Source dataset
uspto-grants-2011_01
Patent number
US07863266B2

Reaction notes

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