HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 178423470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | ethyl 4-chloro-6-methylquinoline-3-carboxylate | HCID 1479091 | — |
| Product | HCID 178423470 | HCID 178423470 | — |
Reaction Steps
The title compound was prepared following the procedure described in Step 3 using 3f and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm): 2.46 (3H, s), 7.16 (1H, t, J=7.41 Hz), 7.41 (2H, dd, J=8.51, 7.14 Hz), 7.46 (1H, dd, J=8.52, 1.92 Hz), 7.58 (1H, d, J=8.51 Hz), 8.00 (1H, br), 8.21 (2H, dd, J=7.69, 1.10 Hz), 8.66 (1H, s). m/z 276.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863266B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-2ef644655dfb4354926cb434c8657da6 |
| Source note | uspto-grants-2011_01 |